回复：[教程篇]使用分区工具分区U盘并安装PE

你顺序反了
可以先分区，再安装PE的

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rem == CreatePartitions-BIOS.txt ==
rem == These commands are used with DiskPart to
rem create three partitions
rem for a BIOS/MBR-based computer.
rem Adjust the partition sizes to fill the drive
rem as necessary. ==
select disk 0
clean
rem == 1. System partition ======================
create partition primary size=350
format quick fs=ntfs label="System"
assign letter="S"
active
rem == 2. Windows partition =====================
rem == a. Create the Windows partition =======
create partition primary
rem == b. Create space for the recovery image
shrink minimum=15000
rem ** Note, adjust the size to match
rem the size of the recovery image.
rem == c. Prepare the Windows partition ======
format quick fs=ntfs label="Windows"
assign letter="W"
rem == 3. Recovery image partition ==============
create partition primary
format quick fs=ntfs label="Recovery image"
assign letter="R"
set id=27
list volume
exit